SYNTHESIS OF SnO2 NANOCRYSTALS BY SOLID STATE REACTION FOLLOWED BY CALCINATION-中国期刊网

摘要 NanocrystallineSnO2wassynthesizedbydirectmixingandgrindingofSnCI4-5H2OandNaOHatroomtemperature,followedbycalcinationatdifferenttemperaturesfordifferenttimesinair.ProductsampleswerecharacterizedbyX-raydiffractionandtransmissionelectronmicroscope,revealingthattheamorphousprecursorSnO2wastransformedtocrystalsat200℃for3h,andthattheaverageparticlesizeincreaseduponraisingthecalciningtemperatureorprolongingthecalciningtime.Themechanismofthephasetransformationoftheproductsisdiscussed.

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SYNTHESIS OF SnO2 NANOCRYSTALS BY SOLID STATE REACTION FOLLOWED BY CALCINATION

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SYNTHESIS OF SnO2 NANOCRYSTALS BY SOLID STATE REACTION FOLLOWED BY CALCINATION

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