简介：TheballmillingofFe-24MnandFe-24Mn-6Simixedpowdershasbeenperformedbythehighenergyballmillingtechnique.ByemployingX-raydiffractionandMoessbauermeasurements.Theccmpositionevolutionduringthemillingprocesshasbeeninvestigated.TheresultsindicatetheformationofparamagneticFe-MnorFe-Mn-Sialloyswithametastablefccphaseasfinalproducts.whichimplythattheFeandMnproceedaco-diffusionmeenanismthroughthesurfaceoffragmentedpowders.Thethermalstabilityandcompositionevolutionoftheas-milledalloyswerediscussedcomparingwiththebulkalloy,.

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简介：ＣｕｒｉｅＴｅｍｐｅｒａｔｕｒｅｏｆＡｍｏｒｐｈｏｕｓＦｅＳｉＢａｎｄＦｅＷＳｉＢＡｌｏｙｓＷａｎｇＬｉｎｇｌｉｎｇ，ＺｈａｏＬｉｈｕａ，ＨｕＷａｎｇｙｕ（王玲玲）（赵立华）（胡望宇））ＤｅｐａｒｔｍｅｎｔｏｆＰｈｙｓｉｃｓ，ＨｕｎａｎＵｎ...

简介：PositronannihilationbehaviorshavebeenstudiedinthesinglephaseNd2Fe14BmagnetandthenanocompositeNd2Fe14B/α-Femagnet,preparedbymeltspinning.Theresultsshowedthatthenumberofvacancy-clusteratgrainboundariesincreaseswithincreasingannealingtemperatureforthebothtypesofmagnets.Theincreaseofthiskindofdefectcanimprovethecoercivityof

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简介：1.IntroductionSofarthemicrostructureandcoercivityofSm（Co,Cu,Fe,Zr）7.4alloyhavebeenstudiedindetailbyvariousauthors.TheeffectofZr-richlaminarphasestructureonthehighcoecivityofalloyismoreattractive.Thechangesofmagnetic

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简介：由于弱氧化剂(如H~+和Fe~(3+))只能将Fe氧化为Fe~(2+),而强氧化剂(如氧化性酸)首先将Fe氧化为Fe~(3+)、生成的Fe~(3+)又可以被Fe还原为Fe~(2+),加上浓硫酸或浓硝酸与过量Fe反应时酸的浓度在不断降低,导致Fe与酸的反应相当复杂。一、与非氧化性酸的反应发生置换反应,生成Fe~(2+)而不能生成Fe~(3+):

简介：通过实验建立了野外水质Fe2+、Fe3+的测定方法，不用电力和携带仪器设备，目视比色。简便快速，具有较好的准确度。

简介：AnFEanalysisprocedurewaspresentedtopredictthebehaviorofsoilogeogridinterctionunderautomobileloading.Thedynamicinteractionsbetweenthetransversebars,thelongitudinalribsandthesoilweresimulatedbyasystemconsistingofnonlinearsprings,dashpotsandmasses,tostudythedeformationpropertiesofthereinforcedsoil.Theequivalentstiffnessanddampingratioscouldbedeterminedwiththeshakingtable.Thedynamicresponsesofareinforcedsubgradewereanalyzedwiththe3Dfiniteelementapproach.Thisapproachisprogrammedandappliedtoanalyzethesoilogeogridinteractionunderdynamicloading.Thecomparativeanalysisoftheresponseofthereinforcedsubgradeandthatofthesubgradewithoutreinforcementshowsthatthegeogridplacedatthebottomofthebaselayermayeffectivelyreducetheaccumulativeplasticdeformationduetothecyclicautomobileloading.

简介：现行教材中有关Fe(OH)2的制备装置由于是一个开放的反应体系，故实际上只能观察到瞬间的Fe(OH)2白色沉淀(几乎分辨不出)．要较长时间观察到白色沉淀的生成，关键是怎样降低反应体系中氧气的存在量和操作过程中氧气的引入量．笔者在此将几种典型的改进方法作一介绍．

简介：张力爬精细的Fe-Mn二进制合金containing0.42-1.21wt.%Mn的行为从房间温度在温度范围被调查了到475Kunder10-50MPa。张力的测试以紧张率在uniaxail负担下面以经常的小标题速度被执行10(-4)s(-1)。压力代表和激活精力决心澄清变丑机制。稳定的状态的获得的变化爬关于为Fe-Mn二进制合金的应用压力的率在大约20MPa展出二不同政体，显示一个可能的变化在爬机制。平均压力代表是约2.2，它是在合金滑动的谷物boundry的一个特征。为塑料流动的激活精力从135～92kJ/mol变化，取决于Mn内容。

简介：ThedetailedmicrostructuresofNi80Fe20/Fe50Mn50superlatticeshavebeencharacterizedusingbothx-raydiffractiontechniquesandtransmissionelectronmicroscopy.Theobrivouslayeredstructure,typicalcolumnstructureandtwinswhichexistinNi80Fe20/Fe50Mn50superlatticeswereobservedthroughperformingtransmissionmicroscopy.Bycombiningthetechniqueoflowanglex-rayreflectivity(specularandoff-specularscans)withtheanomalousscatteringeffectandhigh-anglex-raydiffraction(usingconventionalx-ray),wequantitativelyanalysedthemicrostructuralvariationasafunctionofannealingtemperature.Itisfoundthatthelateralcorrelationlength,the(111)peakintensityofthesuperlatticesandtheaveragemultilayercoherencelengthallincreasewithariseinannealingtemperatureannealingcandecreasetherootmean-squareroughnessattheinterfacesofNi80Fe20/Fe50Mn50superlattices.theobtainedmicrostructuralknowledgewillbehelpfulinunderstandingthemagneticpropertiesoftheni80Fe20/Fe50Mn50exchangebiassystem.

简介：WehavemeasuredthedeepenergyleveloftheInP:Fewhichissemi-insulatorthroughthemethodofOTCS.TheeffectoflightintensityonOTCSmeasurementismainlydiscussed.ThereareelectrontrapofET=0.034eVandholetrapofET=1.13eVinInP:Feunderthestronglightandlowtemperature.ThelocationoftheOTCSpeakofelectrontrap(ET=0.34eV)movestowardsthedirectionofhightemperaturer,whenthelightintensitywasincreased,ETisdifferentunderdifferentlightintensity.Itiscorrectedintermsoftheorythatthestuffratioofthedeepenergylevelisaffectedbythelightintensity.Theexperimentsshowthattheerrorisdecreasedgreatlywiththecorrection.

简介：本文采用溶胶-凝胶法，获得了铁掺杂的纳米TiO2样品，XRD和透射电镜测量表明在600℃以下焙烧时为锐钛矿，颗粒度在10nm以下，样品在1000℃下焙烧时，转变为金红石相，颖粒度增大。EXAPS和穆谱表明，铁的确掺杂到TiO2晶格内，表现为3价。铁的掺杂改变了纯的TiO2的性质，对于锐铁矿相的掺铁纳米TiO2，其紫外-可见反射光谱给出在481nm处出观了新的吸收峰，；对于以金红石相为主的掺铁纳米TiO2，其紫外-可见反射光谱在512nm处出现了新的吸收峰。

简介：通过水热法合成了骨架含铁的杂原子丝光沸石，采用XRD，FT－IR及TPR等表征技术确认铁进入了分子筛骨架。利用XAFS技术对分子筛中铁的精细结构和配位环境进行了表征和计算，近边吸收的Fe-K边前跃迁证实铁在分子筛骨架中位于四面体配位环境中，与邻近原子存在共价键作用；铁－氧配位键长为0.188-0.189nm.

简介：ThebasestructureofinsituTiCP/Fecompositesfabricatedunderindustrialconditionwaschangedbydifferentheattreatments.Erosiveweartestswerecarriedoutandtheresultswerecomparedwiththatofwear-resistantwhitecastiron.TheresultssuggestthatthewearresistanceoftheinsituTiCp/Fecompositeishigherthanthatofwear-resistantwhitecastironunderthesanderosivewearcondition.Thewearmechanismofthewear-resistantwhitecastironwasacycleprocessthatbasesurfacewaswornandcarbideswereexposed,thencarbideswasbrokenandwearpitsappeared.WhilethewearmechanismofinsituTiCp/FecompositewasacycleprocessthatbasesurfacewaswornandTiCgrainswereexposedanddropped.ThewearresistanceofinsituTiCp/Fecompositewaslowerthanthatofwear-resistantwhitecastironundertheslurryerosivewearcondition.Undersuchcircumstance,thematerialwasnotonlyundergoneerosivewearbutalsoelectrochemistryerosionduetothecontactwithwaterinthemedium.Thewearbehaviourscanbeacombinationoftwokindsofwearandthesanderosivewearisworsethanslurryerosivewear.

简介：Magnetizationanddemagnetizationcurvesandhysteresisloopsapplieddifferentmagnetizing.fieldsinsinteredNd-Fe-BandNd-Dy-Fe-Bmagnetsfromthermallydemagnetizedanddcfield-demagnetizedstateswereinvestigatedattemperaturesofupto150℃.Thefirst-quadrantremagnetizationcurvesandthecurvesofcoerciveforces_MH_CversusrernagnetizingfietdsH_mfromdcfield-demagnetizedstateatroomtemperatureshowasteparoundmagnetizingfieldasabsolutevalueofthemaximumintrinsiccoercivity.Thestepsof_MH_C-H_mcurvesshiftedtolowerremagnetizingfieldsandtheshapesofmagnetizationcurveschangedfromsteptypetoprecipitoustypewhentemperaturewentupto100～150℃orafterthespecimenwasthermallydemagnetizedatatemperaturehigherthantheCurietemperature.Thesteepriseofkneecoereivitywithincreasingmagnetizingfieldisbehindthatof_MH_C.NotethatthemagnetichardeninginsinteredNd-Fe-Bmagnetsiscontrolledbypinningofdomainwalls.

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简介：NitridingisemployedforthehardFeelectrodepositiontoproduceahard-facingandantiwearcoating.Itonlytakes1hforthehardFecoating,whichismuchshorterthannitridingtheFeandsteel.Theresultsshowedthatthenitridingcanincreasethemicrohardness,wearresistanceofthecoating,aswellasthebondingstrengthofthecoatingwiththesubstrate.Additionallyitcaneliminatethebrittleness,turntheinternalstressofthecoatingfromtensiontocompression.ThewearresistanceofthenitridedFecoatingis4.6timesashighasthatofCrcoating.ItissimpleandeconomictocombinehardFeelectroplatingandnitriding,whichisagoodtechnologyofthetribologicalsurfacemodification.