简介：Rod-likeZnOparticlesweresynthesizedviaasol-gelmethodbyaddingethylenediamine(EDA)tothereactionsystemofZn(Ac)2·2H2OandH2C2O4·2H2O.ThecrystalphaseandmorphologyoftheproductswerecharacterizedbyXRD(X-raypowderdiffractometer)andTEM(transmissionelectronmicroscope).Rod-likeZnObelongstothehexagonalWurtzitesystem,withdiametersandlengthsofabout20-200nmand0.2-1.5m,respectively.Experimentalresultsshowedthatthemorphologyofnano-ZnOcanbecontrolledbymodulatingthequantitiesofEDAaddedintothereactionsystemandthatEDAplaysanimportantroleintheformationofrod-likeZnOparticles.Thegrowthmechanismoftherod-likenanoZnOwasbrieflydiscussed.Theproposedfacile,reproducible,effectiveandlow-costsynthesispromisesfuturelarge-scalepreparationofnanostructuredZnOforapplicationinnanotechnology.

简介：ZnOnanoparticleswithverynarrowsizedistributionweresynthesizedbycouplinghomogeneousprecipitationwithmicroemulsionunderpulsedmicrowaveheating.TheconditionsofpreparingZnOnanoparticleswereinvestigated.TheproductswerecharacterizedwithDTA,TGA,XRD,TEMandUV-Vis.ThesynthesizedZnOnanoparticeshadmuchstrongerultravioletabsorptivitythannormalZnOpowders;theaveragesizeofproductswassensitivetothevariationofthepowerordurationofmicrowaveirradiation.

简介：TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn（OH）2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe（100）planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration（O-H…O）,therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.

简介：锁泉华的microfibrous网络由8m(dia)的3vol.%组成镍microfibers被利用了骗诱100200mdia的30vol.%。多孔的Al2O3。ZnO和CaO然后被早期的湿受精方法高度驱散到骗诱的Al2O3的毛孔表面上。由于表面区域，毛孔尺寸/粒子尺寸，热传导性，和空体积的唯一的联合，当在甲醇蒸气改过使用了时，产生microfibrous催化剂composites提供了催化的床反应和利用效率的重要改进。粗略地甲酸盐的260mL/min，包括>70%H2，<5%公司和踪迹CH4，与>97%甲醇变换，能在我们骗诱的新奇microfibrous的1cm3床卷被生产在470湩瑡潩?潰祬敭r合成的ZnO-CaO/Al2O3催化剂?鑈я鑈я8

简介：针对＂FBAR（薄膜体声波谐振器）-梁＂结构悬臂梁厚度不足、＂嵌入式FBAR＂结构微加工工艺复杂的缺点,提出了新型＂膜片上FBAR（FBAR-on-diaphragm）＂结构的微加速度计。其弹性膜片由氧化硅/氮化硅复合薄膜构成,既便于实现与硅微检测质量和FBAR的IC兼容集成加工,也利于改善微加速度计的灵敏度和温度稳定性。对由氧化硅/氮化硅双层复合膜片-硅检测质量惯性力敏结构和氮化铝FBAR检测元件集成的膜片上FBAR型微加速度计进行了初步的性能分析,验证了该结构的可行性。通过有限元模态分析和静力学仿真得出惯性加速度作用下膜片上FBAR结构的固有频率和弹性膜片上的应力分布;选取计算所得的最大应力作为FBAR中压电薄膜的应力载荷,结合依据第一性原理计算得到的纤锌矿氮化铝的弹性系数-应力关系,粗略估计了惯性加速度作用下氮化铝薄膜弹性系数的最大变化量;采用射频仿真软件,通过改变惯性加速度作用下弹性常数所对应的纵波声速,对比空载和不同惯性加速度作用下加速度计的谐振频率,得到加速度计的频率偏移特性和灵敏度。进一步分析仿真结果还发现：氧化硅/氮化硅膜片的一阶固有频率与高阶频率相隔较远,交叉耦合小;惯性加速度作用下,谐振频率向高频偏移,灵敏度约为数kHz/g,其加速度-谐振频率偏移特性曲线具有良好的线性。