简介:6-chloro-3-nitrotoluene-4-sulfonic酸(CNSA)的Photocatalytic减小面对甲醇和表面活化剂在紫外照耀TiO2暂停被学习。CNSA,TiO2,水,添加剂和表面活化剂的混合物与一件夹克衫被放进一个石英玻璃反应堆,它在氮气体清除用一盏高压力Hg灯被照耀。与甲醇,CNSA的变换从7.7%~34.6%增加了。三表面活化剂显著地在钠dodecylbenzenesulfonate(DBS)的减少的顺序支持了photocatalytic减小变换,cetyltrimethylammonium溴化物(CTAB)和钠dodecylsulfate(SDS)。在分别地包含DBS和CTAB的暂停,CNSA变换与甲醇与吸附比率在坚固性增加了,但是没有甲醇,与吸附比率相反地变化了。但是对吸附比率的明显的影响都没被观察与或没有当SDS集中是批评micelle集中(cmc)时,增加的甲醇。CNSA的photocatalytic减小面对甲醇和表面活化剂在紫外照耀TiO2暂停被提高。甲醇高效地禁止了photogenerated洞和电子的再结合。在1cmc附近的表面活化剂导致了最高的减小变换。
简介:测定无机化工产品中的N(NH^+4)、Cl的含量,若将甲醛法和莫尔法相结合,则有以下特点:(1)快速经济,分析条件易于控制;(2)实现了NH^+4的分析和掩蔽一次完成;(3)有较好的精密度和准确度,可以在一定范围内进行试用。
简介:工程教育实践教学改革要从工程人才培养的目标出发,把握其职业性、工程性和现场性等实践教学特征;要遵循学生本位、职业导向、系统化培养、彰显特色、国际视野五项基本原则,推进实践教育教学改革;要围绕确立合适的目标体系、构建合理的课程内容体系、创新实践教学模式、改革管理体制机制和建立实践教学保障机制等多个层面,探索实践教学体系构建的路径。
简介:Longlastingstrontiumaluminatephosphorsweresynthesizedbymeansofcoatedprecipitationintheexperiment.SrA12O4monoclinicphasewithlongafterglowwassynthesizedat1100℃withtheaidofH3BO3,andthesynthetictemperaturedecreasedabout100℃-150℃thaninsolidstatereaction.TheprocessofheattreatmentwasstudiedbyTG-DTA.ThephasecompositionsofpowderswereanalyzedbyXRD.ThemicrographsofthesampleswereinvestigatedbySEMandtheluminescentpropertieswereresearchedbyopticalspectrum.TheeffectsofH3BO3onthephasecompositionandmicrostructureofthecalcinedpowderswereinvestigated.TheresultsindicatedthatH3BO3acceleratedtheformationofSrAl2O4byconsumingtheintermediatephase.TheadditionofDy2O3stimulatedtheafterglowpropertyduetotheincreaseinthedepthofthetrapcenterinthematerials.
简介:TheeffectofMnsubstitutionforpartialFeinRFe11Tionstructureandmagneticpropertiesofcompoundswasresearched.RFe7Mn4Tisamples(R=Y,Tb,Dy,Ho,Er)werepreparedbymeansofvacuumarc-meltingandsubsequentvacuumannealing.ThestructureandmagneticpropertiesofRFe7Mn4TicompoundswereinvestigatedbyX-raypowderdiffractionandmagneticmeasurements.Thefollowingconclusionswereobtained:alltheRFe7Mn4TicompoundscrystallizeintheThMn12-typestructure.Thelatticeconstantsandtheunit-cellvolumechangedwiththeincreaseofatomicnumberforR=Y,Th,Dy,Ho,andEr.ThecompensationcharactersappearfortheDyFe7Mn4TiandHoFe7Mn4Ticompounds,andthecompensationtemperatureswereabout123Kand90K,respectively.TheCurietemperature,thesaturationmagnetization,andsaturationmomentofRFe7Mn4Ticompoundsweregiven.