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63 个结果
  • 简介:CurieTemperatureofAmorphousFeSiBandFeWSiBAloysWangLingling,ZhaoLihua,HuWangyu(王玲玲)(赵立华)(胡望宇))DepartmentofPhysics,HunanUn...

  • 标签: CURIE TEMPERATURE FeSiB and FeWSiB ALLOYS
  • 简介:InordertocontrolthesizeanddistributionofthehighconductiveFe2PinLiFePO4/Fe2Pcomposite,twodifferentcoolingrates(Fast:15℃·min-1,Slow:2℃·min-1)wereemployedaftermechanicalalloying.Thedischargecapacityofthefastcooledwas83mAh·g-1andtheslowcooled121mAh·g-1.TheparticlesizeofthesynthesizedpowderwasexaminedbytransmissionelectronmicroscopyanddistributionofFe2Pwascharacterizedusingscanningelectronmicroscopy(SEM).Inaddition,two-stepheattreatmentwascarriedoutforbetterdistributionofFe2P.X-raydiffraction(XRD)andRietveldrefinementrevealthatLiFePO4/Fe2Pcompositeconsistsof95.77%LiFePO4and4.33%ofFe2P.

  • 标签: LiFePO4/Fe2P COMPOSITE mechanical ALLOYING HEAT treatment
  • 简介:Sinceamorphousalloyshavewiderapplication,theycannotbefabricatedusingtheconventionalcoolingvelocity.ThebarmaterialplasmasprayingisadoptedtofabricateFebaseamorphousalloyinthisinvestigation.Thecrystallizationdegree,microstructure,micro-hardness,composition,crystallizationtemperatureoftheamorphousalloyandtheflyingrulesoftheatomizedparticlesintheprocessoftheplasmasprayaretested.Theresultsshowthatthealloypreparedhasthehighamorphousdegreeandhomogeneousmicrostructure,micro-hardnessandthecrystallizationtemperaturecanreach1187HVand531℃respectively.Theatomizationisverywellduringtheprocessofplasmaspraying;andthereishighthermalgradient,thecoolingvelocityreaches6.07×107K/s.

  • 标签: 非定形合金 棒材 等离子体喷射 焊接
  • 简介:磁性的元素Fe,公司和Ni的线性热扩大(CLE)的系数用与MATLAB计算相结合的理论模型从试验性的信息被估计。模型参数能精确地被决定,并且估计的数据在对试验性的结果的好同意。便于评价,热扩大的理论被使用把CLE分开成它的无磁性、磁性的部件。对CLE的无磁性的贡献的计算基于MnBi/NdFeB混血儿的修改Grc性质结合的磁铁都逐渐地减少,当混合磁铁的密度几乎线性地改善时。在293-398的一个温度范围?K,混合磁铁的coercivity温度系数从0.59逐渐地改善?%比较。建模和频率与二低角落频率认为压力消除阀门是一个秒顺序系统是合理的试验性的结果表演。PID控制,死了的乐队赔偿控制和鷸?鷸??

  • 标签: 线性热膨胀系数 磁性元件 评估 模型参数 实验数据 MATLAB
  • 简介:ThesolidsolubilityofCe、La、SmandNdinFeorNiatvarioustemperaturewasdeterminedbymeansofadiffusion-couplemethodwiththeaidofanelectronprobemicroanalyzer.Twomethods,namelyareamethodandwholerangemethod,wereproposedfordataprocessinginthepresentpaper.Theprincipleandre-latedproblemsintheexperimentaldeterminationofthesolidsolubilityofrare-earthelementsinFeorNibyuseoftheabovementionedmethodswerealsodiscussed.

  • 标签: Solid SOLUBILITY RARE earths FE NI
  • 简介:这份报纸的主要注意被奉献给在多晶的Fe82Ga18样品。合金用钮扣弧融化被融化并且在water-cooled铜模子团结了。光显微镜(OM)结果在团结微观结构证实大圆柱的谷物的发展。阶段宪法和样品的磁性的领域结构被X光检查衍射(XRD)和磁性的力量显微镜学(MFM)学习。结果为由定期排列的磁性的域组成的样品与A2结构显示出一个单相的稳固的解决方案。尽管一些像迷宫的子域在很少区域被发现,排列得好的像条纹的领域是在样品的占优势的模式。它在团结期间在一个比较喜欢的结晶的方向之上表明谷物形态学和磁性的领域结构的高依赖。

  • 标签: GALFENOL 团结质地 谷物形态学 磁性的领域结构
  • 简介:ArapidlysolidifiedAl-2.5Ti-2.5Fe-2.5Cr(massfractionin%)alloywaspreparedbymeltspinning.Asquenchedandas-annealedmicrostructureswerestudiedbyX-raydiffractometry(XRD),transmissionelectronmicroscopy(TEM),high-resolutiontransmissionelectronmicroscopy(HREM)andenergydispersivespectrum(EDS)analysis.Themicrohardnessofthealloyatdifferentannealingtemperatureswasmeasured.TheresultsobtainedindicatethatthemicrohardnessoftherapidlysolidifiedAl-2.5Ti-2.5Fe-2.5Cralloydoesnotvarywithdifferentannealingtemperatures.Theas-quenchedmicrostructureofthealloyincludestwokindsofdispersedprimaryphases:Al3TiandAl13(Cr,Fe)2.Afterannealingat400℃for10h,thestablephaseAl13Fe4appearsinthemicrostructure.

  • 标签: Al-Ti-Fe-Cr合金 微结构 热稳定性
  • 简介:ThehydrogenstoragepropertiesofTi1.2Fe+xCa(x=1%,3%and5%inmassfraction)alloyswasinvestigated.ResultsshowthatthemodifiedalloyscanbeactivatedwithoutanythermaltreatmentatroomtemperatureduetotheadditionofCaandexcessTiinthealloys.HydrogenstoragepropertiesofthesemodifiedalloysvarywithCaamountandreactiontemperature.Inaddition,theinfluencemechanismoftheadditionofCaandexcessiveTiontheactivationbehaviorandhydrogenstoragecapacityofthealloyswasdiscussed.

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  • 简介:利用平衡合金法,采用扫描电镜-能谱仪和X射线衍射方法对Al-Fe-Sn三元系973和593K等温截面的相关系进行实验测定。实验结果表明:在此两个截面上均未检测到三元化合物;973K时液相中Fe的最大固溶度为1.6%(摩尔分数),而593K时Fe和Al在液相中的最大固溶度分别为0.6%和5.1%(摩尔分数);在973和593K等温截面上,Sn在Fe-Al化合物中的最大固溶度分别为4.2%和2.3%(摩尔分数);Fe-Al化合物均能与液相保持平衡。

  • 标签: Al-Fe-Sn三元系 相图 固溶度
  • 简介:ThefrictionandwearbehaviorofFe-Alintermetallicsbasedcoatingproducedbyhighvelocityarcsprayingtechniqueunderdryslidingatroomtemperaturewereinvestigatedusingaball-on-disctribotester.Theeffectofslidingspeedonfrictioncoefficientandwearofthecoatingwasstudied.Thewornsurfaceofthecoatingwasanalyzedbyscanningelectronmicroscope(SEM)toexploreslidingfrictionandwearmechanism.Theresultsshowthatthevariationsoffrictioncoefficientcanbedividedintothreedistinctstepsduringthetrail.Boththefrictioncoefficientandthewearofthecoatingincreasewithincreasedslidingspeedduetoacceleratedcrackpropagationrateandlamellarstructurewithpoorductilityofthecoating.Thecoatingsurfaceissubjectedtoalternatelytensilestressandcompressionstressduringslidingwearprocess,andthepredominantwearmechanismofthecoatingsappearstobebrittlefractureanddelamination.

  • 标签: Fe-Al涂层 高速电弧喷涂 滑动磨损 SEM HVOF SHS
  • 简介:TheeffectsofheattreatmentsonthephasetransformationbehaviorofTi49Ni49.5Fe1V0.5andTi48Ni48.5Fe1V2.5alloyswereinvestigated.TheresultsindicatethatthealloyssubjectedtodifferentheattreatmentshaveB2structureatroomtemperature.AllthespecimensexhibitatwostageB2→R→B190martensitictransformationoncooling,butaB190→B2one-stagereversemartensitictransformationonheatingexceptagedA1alloy,whichundergoesanabnormaltwo-stagetransformationuponheating.ThephasetransformationtemperaturesareaffectedbyheattreatmentsandVcontent,whichcanbeattributedtothevariationofthesecond-phaseparticlescontentinthematrix.

  • 标签: 相变行为 热处理 合金 马氏体相变 B2结构 相变温度
  • 简介:Thestructure,CurietemperatureandmagnetostrictionofPr0.15Tb0.30Dy0.55Fe1.85Cx(x=0-0.1)compoundswereinvestigatedbyX-raydiffraction,avibratingsamplemagnetometerandastandardstraintechnique.AllthesamplesshowentirelyMgCu2-typeLavesphasestructure.ThelatticeparameterandCurietemperatureincreasewithCcontentincreasing.Themagnetostrictionathighmagneticfieldshowsmaximumvalueatx=0.05.

  • 标签: MAGNETOSTRICTION Pr0.15Tb0.3Dy0.55Fe1.85 Laves PHASE
  • 简介:InordertoobtainultrafineNd-Fe-Bpowder,aspray-driedprecursorwastreatedbyreduction-diffusion(R/D)process.And,unliketheconventionalR/Dprocess,calciumreductionthatisacrucialstepfortheformationofNd2Fe14BwasperformedwithoutconglomeratingtheprecursorwithCapowder.Byadoptingthismodifiedprocess,itispossibletosynthesizethehardmagneticNd2Fe14Batthereactiontemperatureaslowas850℃.TheaveragesizeofNd2Fe14Bparticlesthatareuniformlydistributedintheoptimallytreatedpowderwas<<1μm.MostNd2Fe14BparticleswereenclosedwiththinlayersofNd-richphase.TypicalmagneticpropertiesofsuchpowderwithouteliminatingimpurityCaOwereiHc=~5.9kOe,Br=~5.5kG,and(BH)max=~6MGOe.

  • 标签: NDFEB POWDER spray DRYING reduction-diffusion process
  • 简介:X-raydiffraction(XRD)anddifferentialscanningcalorimetry(DSC)wereusedtoinvestigatethecrystallizationprocessofamorphousAl90TMxCe10-x(atomfractionin%;TM=FeorNi;x=3,5)alloys.AgingeffectswereexaminedbyX-raydiffraction.ThestructurecorrespondingtotheprepeakfortheamorphousAl90Fe5Ce5alloyismorestablethantheamorphousmatrix,butitisnotstableforamorphousAl90Ni5Ce5alloyduringthefirstcrystallizationstageandevendecomposesatroomtemperature.AlthoughbothAl-NiandAl-Fehavestrongchemicalbonding,thecrystallizationonsettemperatureofamorphousAl-Fe-CealloysismuchhigherthanthatofamorphousAl-Ni-Cealloys,whichislikelycausedbythedifferentstabilityofthestructurecorrespondingtotheprepeak.ThecrystallizationonsettemperatureincreasesasCe/NiratioincreasesinamorphousAl90NixCe10-xalloys,whereasitdecreasesasCe/FeratioincreasesinamorphousAl90FexCe10-xalloys.AbetteratomicpackingproducesasCecontentincreasesbecauseofthesizemismatchinAlNi-CesystemsandasFecontentincreasesbecauseoftheincreasingFecentralstructuralunits.

  • 标签: 非晶形合金 Al90TMxCe10-x合金 稳定性