简介:Thetenacityofheat-affectedzone(HAZ)willdeclineandthesizeofgrainswillincrease,becauseoftheoverheatingonHAZwhensubmergedarcwelding(SAW)isusedtothickplatewithhighheatinput.TheshapingwillworsenwhenSAWisusedtothinplatewithhighcurrentathighspeed.AnewSAWtechnology,thepulseddirectcurrent(DC)automaticSAW,willbeputforwardinthispaperinordertoovercometheaboveshortcomings.Andapulsedcontrollerwithmicro-controllerunit(MCU)asthecore,nixietube(NT)andkeyboardastheman-machineconversationinterfaceisdeveloped.Themainfunctionsofthepulsedcontrollerincludetheoutputofpulsedweldingcurrentandtheworkingwithtwinwire.Theresearchhaswidelyprospectsinapplicationwithsignificantmeaningsintheoryandpracticalengineering.
简介:Titaniumandtitaniumalloyshaveseveraladvantages,butthecostoftitaniumalloysisveryexpensivecomparedwiththetraditionalmetalmaterials.Thisarticleintroducestwonewlow-costtitaniumalloysTi-2.1Cr-1.3Fe(TCFalloy)andTi-3Al-2.1Cr-1.3Fe(TACFalloy).Inthisstudy,weusedCr-Femasteralloyasoneoftherawmaterialstodevelopthetwonewalloys.Weintroducethemicrostructureandtensilepropertiesofthetwonewalloysfromβsolutiontreatedwithdifferentcoolingmethods.Optica...
简介:Reducingthemanufacturingcostofsolarcellsisnecessarytotheirindustrialproduction.Electrodepositingisaneffective,non-vacuummethodwhichisverysuitableforcuttingthemanufacturingcostofthinfilmsaswellasdevelopingitslarge-scaleindustrialproduction.Inthisstudy,about1-μm-thickCu(In,Ga)Se_2(CIGS)precursorswereelectrodepositedonMo/glasssubstratesinaqueoussolutionutilizingathree-electrodepotentiostaticsystem.Triethanolaminewasusedascomplexingagent,andallparametersofelectrodepositionwerepreciselycontrolled.Afterthat,theelectrodepositedprecursorswereselenizedinaSeatmospherewithdifferentheatingramprates(60and600℃·min~(-1)).High-qualityCIGSfilmswereobtained,andtheircharacteristicswereinvestigatedbyX-rayfluorescence,scanningelectronmicroscopy,energydispersivespectroscopy,X-raydiffraction,Ramanspectraandnear-infrared-visible(NIR-Vis)spectra.Theresultsrevealthattherearemanydifferencesbetweenthepropertiesofthefilmsunderdifferentheatingrates.Finally,CIGSsolarcellswerefabricatedusingafastandaslowheatingrate.Themaximumefficienciesachievedforthefilmsselenizedat60and600℃-min~(-1)are3.15%and0.71%,respectively.
简介:Thegrainsizecontrolofthetungstenpowderisessentialforhighqualitytungstenproductsmaking.Basedonthestudiesonthehydrogenreductionprocessoftungstenoxide,amicrocomputersystemisintroducedtothereductionprocessparameterscon-trol.Themicrocomputerprocesscontrolsystem,whichisnowrunninginZhuzhouTungstenandMolybdenumMaterialsPlant,controlstheprocessparametersincludingthetemperatureofthereductionfurnaceandthepressureofhydrogen.Italsocontrolsamechanicalpusherwhichpushstheboatschargedwithbluetungstenoxideintothefurnacetubes.Someofthetechniqueprob-lemsappearedinthereductionprocessandtheprocesscontrolareanalysedinthispaper.Theresultoftheexperimentisalsogiven.
简介:Oxidationprocessoflanthanumhexaboride(LaB6)ceramicpowderwasinvestigated.TheLaB6powdersampleswereheatedcontinuallyfromroomtemperatureto1473Kataheatingrateof10K/minbydifferentialscanningcalorimetry.Theoxidationtestswereconductedatdifferentexposuretemperatures.ThephasesandmorphologiesofthesamplesbeforeandafterexposurewereanalyzedbyXRDandSEM.Itwaspointedoutthatbefore1273K,LaB6hashighoxidationresistantability,whichwasduetothattheoxidelayerhinderstheoxygendiffusionfromoutertothesurfaceofLaB6grains.Theoxidelayerwascomposedofthetransitionphases,whichwerecomposedofLa2O3andB2O3formedfromtheinitialoxidation;whentheoxidationtemperatureexceeded1273K,protectivelayerwasdestroyedduetothevaporizationofliquidB2O3.BasedontheresultsofX-raydiffractionanalysis,oxidationprocessofLaB6ceramicpowdercanbedescribedasfollows:Before1273K,lanthanumborate,La(BO2)3wasformedonthesurfaceofsamples,thenlanthanumoxide(La2O3)andboronoxide(B2O3)werepresentonthesurfaceofsamplesoxidizedwhenthetemperaturereachedto1473K.
简介:Yttriastabilizedzirconia(YSZ)haswidelybeenusedaselectrolyteinsolidoxidefuelcell(SOFC).ThemicrostructureofYSZrelatedtothefabricationprocesswasdiscussedinthepaper.WithYSZnano-powdersabout40-100nmasrawmaterial,theYSZadobewasmanufacturedbytapecalenderingprocess.Thenamedthree-stepsinteringprocesswasperformedat1000℃for2h,thenraisedthetemperaturewithnormalrateandassoonasupto1400℃,thefurnacewascontrolledat1250-1300℃for10-20h.ThehighdenseYSZswiththerelativedensityof96%-99%wereobtained;thegrainsizeofYSZcouldbereducedto0.5-3μm.Theaboveresultisbenefitedtoco-firedintheelectrode-supportedSOFCs.
简介:CalciumhydroxytitanateformedinBayerdigestionprocessofchinesediasporicbauxitewasstudied.InterplanarspacingsofcalciumhydroxytitanatecrystalweredeterminedbyXRDanalysis.Onlyoneendothermicpeakoccursat550~560℃ontheDTAcurveofthiscompound.IRspectrometrystudyhasrevealedthathydroxyldoesexistincalciumhydroxytitanateinsteadofcrystalwater.ObservationunderSEMhasindicatedthatitscrystalgrainsareintheshapeofregularhexagonalplateswith2~8μminedgelengthandlessthan1μminthickness.TheinfluencesofvariousdigestionconditionsontheformationandtransformationofcalciumhydroxytitanateandotherCa-Ti-containingcompounds,suchaslimeaddition;contentanddistributionstateofTiO2inbauxite;digestiontemperatureandretentiontime,werefurtherstudied.
简介:Weldingtechnologyinoil-fieldconstructioninChina¥HOUXianzhong(DaqingOilField)Abstract:Thispaperintroducestheapplicationanddeve...
简介:Throughtheinvestigationontraditionalarcstudweldingprocess,anewweldinggunanditscontrolsystemweredevelopedinthispaper.Thesteppingarcstudweldinggunwasmainlymadebyasteppingmotorasactuatingunitandascrew-drivendeviceasmovingunit.AcontrolsystemwithaMCS-51single-chipmicrocomputerasmaincontrolcomponentwasusedtorealizethenewstudweldingprocedure.Thisnewweldingprocesswithsteppingstudweldinggunisnamedassteppingarcstudwelding.Inthenewweldingprocess,thestudactioncanbelookedasconstitutedbysomemicrosteps.Thesettingandadjustingofthesteppingarcweldinggunbehaviorparametersareaccomplishedindependently.Itisindicatedfromtheresultsofprocesstestsandbendingtestthatthesteppingarcstudweldingprocessispracticable.
简介:ElectrodeProcessofY(Ⅲ)onNickelElectrodeandSurfaceMetallizingZhouChungen(周春根)(UniversityofAeronauticsandAstronauticsBeijing,Be...
简介:Adetailedanalysisofthecathodeprocessduringtheformationandgrowthofthetitaniumdepositonthewirescreenbasketinconnectionwithaconsiderationofthecurrentefficiencyisgiveninthepresentpaper.Theequationsdescribingthedistributionofcurrentdensities,titaniumionconcentrationalongthedepositlayerandtheequationofthetheoreticalcurrentefficiencyhavebeenderivedanddiscussed.Onthebasisoftheseequationsandtheexperimentalresultsoftitaniumelectrolysisthereasonandmechanismforlossofcurrenthasbeenascertainedtobeattributedtothedischargingofsodiumandlowvalentsodiumionsontheoutsidelayerofthecathode.
简介:ProcessDevelopmentAspectsofAluminium-TitaniumMasterAlioysKrishnanT.S.;RajagopalanP.K;andBoseD-K.(Metallurgy.Division,BhabhaAt...
简介:Anovelprocesswasproposedforrecoveringnickelfromnickeliferouslateriteores.Firstofall,siliconandmagnesiumwereremovedfromlateriticorebyhighconcentrationsodiumhydroxideleachingandcarbonationrespectively,soastoenrichnickel.Thenthemethodofammoniacarbonateleachingwasadoptedtorecovernickelfromthecarbonizedslag,andtheremainingresiduewasusedasarawmaterialforrecoveringiron.Theeffectsoftemperature,ammoniacarbonateconcentration,liquid/solidratioandstirringspeedontherecoveryofnickelwereexamined.Whentheleachedresiduereactedwithammoniacarbonate(6mol·L-1)inaratioofliquid-to-solidof5-1at60℃for150minatthestirringspeedof300r·min-1,approximatemorethan95%nickelwasrecovered.Duringthewholeprocess,therewasnocontaminationproducedandthechemicalrawmaterialswererecycled,thustheprocesswasagreentechnologythathavinggoodsocialbenefit.