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简介：The1.3-dipolarcycloadditionreactionof2-trifluoromethyl-oxazoloneandtheactivatedcarbon-carbonmultiplebondwasstudiedandgaveaconvenientwaytosynthesize2-trifluoromethylpyrrolederivatives.

简介：Basedonloadseparationtheory,theloadseparationparameterSpbmethodisaneffectiveapproachforestimatingtheJ-resistancecurvefromrecordsofloadversusdisplacementdirectly,usingonesharpcrackedspecimenandanadditionalreferencebluntcrackedspecimen.However,theeffectofthereferencebluntcrackedspecimenonJ-resistancedeterminationwasnotexplicitlyconsideredinpastwork.Inthispaper,amodifiedloadseparationparameterSpbmethodwasdevelopedtoeliminatethiseffect,andthenauniqueestimationofinstantaneouscracklengthforonesharpcrackedspecimencouldbeobtained.Furthermore,aforcedbluntingcalibrationmethodwasalsoadoptedtodeterminetheinstantaneouscracklengthintheloadinseparableregion,referringtoanormalizationmethod.ExperimentsonsteamturbinerotatorsteelCr2Ni2MoVwerecarriedouttoestimateJ-resistancecurvesusinganunloadingcompliancemethod.Byremovingunloadandreloaddatafromload-displacementrecords,theJ-resistancecurveforthesamesharpcrackedspecimenwasestimatedusingthemodifiedseparationparameterSpbmethod.TheresultsindicatethatthemodifiedSpbmethodcompletelyeliminatestheeffectofthereferencebluntcrackedspecimenontheinstantaneouscracklengthdeterminationofthesharpcrackedspecimen.However,differentJ-resistancecurvesinasmallrangeofcrackextensionarepresentwhendifferentbluntingcoefficientsareusedinthebluntinglineequation.TheJ-resistancecurveobtainedfromthemodifiedSpbmethodagreeswellwiththatobtainedfromthecompliancemethod.

简介：热行为，机制和在一个规划温度的模式的标题混合物的发热的第一阶段的分解反应的运动参数借助于DSC，TG-DTG和红外被调查了。反应机制被建议。在微分形式，明显的激活精力(Ea)和这反应的pre指数的因素(A)的实验运动模型功能是(1-)?1.119，211.3kj/mol和1020.2s?1分别地。混合物的热爆炸的批评温度是202.2爠慥瑣潩?㈠低??湡敧漠??????????????鈿酌顛鱎?????疞????陴?陴?T

简介：以4-[（8-羟基-5-喹啉）偶氮]-苯磺酸与氯化钴为原料,采用溶剂热法通过原位反应合成{[Co（5-氨基-8-羟基喹啉）_2]·H_2O}_n,并通过X-射线单晶衍射方法确定了该配合物的晶体结构.结构分析表明：标题配合物属于斜方晶系,Pbcn空间群,晶胞参数a=1.321（2）nm,b=0.811（2）nm,c=1.511（2）nm,α=β=γ=90.00°,V=1.619（3）nm~3,Z=4,R_1=0.0516,wR_2=0.1025.配合物中存在ππ堆积相互作用和氢键作用,将配合物连接形成三维超分子网络结构.

简介：Inthiswork,syngasmethanationoverNi-W/TiO2-SiO2catalystwasstudiedinafluidized-bedreactor(FBR)anditsperformancewascomparedwithafixed-bedreactor(FIXBR).Theeffectsofmainoperatingvariablesincludingfeedstockgasesspacevelocity,cokecontent,bedtemperatureandsulfur-tolerantstabilityof100hlifewereinvestigated.ThestructureofthecatalystswascharacterizedbyXRD,N2adsorptiondesorptionandTEM.Itisfoundthatundersamespacevelocityfrom5000h1to25000h1FBRgaveahigherCH4yield,lowercokecontent,andlowerbedtemperaturethanthoseobtainedinFIXBR.Ni-W/TiO2-SiO2catalystpossessedexcellentsulfur-tolerantstabilityonthefeedstockgaseslessthan500ppmH2SinFBR.ThecarbondepositsformedonthespentcatalystwereintheformofcarbonfibersinFBR,whileintheformofdenseaccumulationdistributionappearanceinFIXBR.

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简介：作者在C上给围住的双线性的表格的Fourier变换的描述*(S1)×C*(二基础半的S2)以乔丹组织S1和S2*-representations,hemimogeneous随机域，并且象一样微弱地，harmonizable随机S回答1和S2直到Hilbert空格。

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简介：一系列1-[2-(2-methoxyphenylthio)本甲基]-4-arylpiperazines衍生物基于5-HT1A/SSRI药设计策略被设计并且综合。综合混合物为他们的双5-HT1A/5-HTT活动被评估。

简介：三角函数问题和解三角形问题是江苏高考的必考内容，也是学生的拿分点，但学生在做此类问题的时候往往会由于错误的分析思路而导致失分．通过角度之间的变换，探求角度之间的关系从而求角的三角函数问题是高考的重点考察范围，那么掌握这一块的运算技巧和解题方法是学生的首要任务，笔者在上一节普通的习题讲评课时，学生对一个问题的思维方式和思维模式给笔者留下了深刻地印象．

简介：【本节需学习的内容】本节教材由“光由空气射入水中时的折射情况”和“光通过玻璃砖时的折射特点”两部分组成，主要是通过实验观察光的折射现象和折射的特点．

简介：【本节需学习的内容】本节教材由“长度的单位及测量”、“时间的单位及测量”两个部分组成，介绍长度的特殊测量方法以及长度和时间的估测．

简介：教学是要“教会学生学”，那要教会学生学什么呢？笔者认为首先要“教学生‘提出’问题”．那又该怎么教？经过十几年的教学经验，笔者认为可以通过适当的情境启发学生提出问题．这个情境要靠教师创设，只有教师创造性的教，学生才能创造性的学．笔者以一道“形散而神似”的习题为素材，进行了一次教学尝试．以下是这节课的片段实录以及一些不成熟的思考，仅供参考．

简介：Lithium-aluminum-cobalt-nickeloxideLiAlxCoyNi1xyO2particles,generallyusedascathodeoflithiumbattery,werepreparedbychemicalcoprecipitationfromanaqueoussolutionofLiOH,Al(NO3)3,Co(NO3)2andNi(NO3)2withNH4OH.XRD,SEMandFTIRwereusedtoexaminetheeffectofnickelcontentontheproduct.FTIRpatternsshowedthatincreaseinnickelcontentdecreasedtheabsorptionstrengthofthepeakofspinelstructureoftheproduct,attributedtotheoccupationbynickelinthealuminumsites.Particlesizeandelectricalpropertiesofthelithium-aluminum-cobalt-nickeloxide(abbreviatedasLACNO)particleswerealsodetermined.

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简介：JUNA(JinpingUndergroundlaboratoryforNuclearAstrophysics)isplaningtomeasurethe13C(α,n)16OandsomeotherimportantreactionsatorclosetostellarenergiesusingintenseheliumbeamoutofanECRdrivenacceleratorinJinpingUndergroundlaboratory[1].Deuteriumimpurityinionsourcewillproducessignificantamountofneutrons,limitingthebackgroundlevel.Tocontrolthedeteriumimpurity,wehavedevelopedamethodtomeasurethedeuteriumimpuritywithinHeliumbeamusingthed(d,p)treaction.

简介：LetCdenotethesetofallk-subestsofann-set.AssumeAlohtaininCa,andAlohtainin(A,B)iscalledacross-2-intersectingfamilyif|AB≥2forandA∈A,B∈B.Inthispaper,thebestupperboundsofthecardinalitiesfornon-emptycross-2-intersectingfamillesofa-andb-subsetsareobtainedforsomeaandb,AnewproofforaFrankl-Tokushigetheorem[6]isalsogiven.