简介:对防化研究院某研究所生产的SY-2型CR39探测器与美国Battelle公司生产的CR39探测器进行了快中子灵敏度对比和SY-1型CR39探测器与日本CR39探测器进行了α粒子注量与径迹密度线性关系对比。实验结果证明:防化研究院某研究所生产的CR39探测器与国外同类产品具有相同的快中子灵敏度和同样较好的α粒子注量与径迹密度线性关系,其性能和国外同类产品基本相同。
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简介:TheevaluationofcreepdamagesofCr-Mo-Vsteelusedinthegasturbineofpowerplanthasbeencarriedoutusingtheline-focus-beam(LFB)acousticmicroscopy.Thevelocityofleakysurfaceacousticwave(LSAW)propagatednearthespecimensurfacewasusedforthequantitativeevaluations,whichwasmeasuredbyLFBacousticmicroscopyusingthev(z)curveanalysismethod.IthasbeenshownthatwiththeincreaseofcreepdamagefractionofmetalmaterialtheLSAWvelocitydecreasesobviously,whichsuggeststhepossibilityofnondestructiveandquantitativeevaluationsofcreeddamagesinmetalmaterialsbyacousticmicroscopy.
简介:【摘要】 : 目的 分析探讨 CR、 CT、 MRI在脊柱结核诊断中的临床价值。方法 选取 2018年 12月 ~2019年 8月收治的 84例脊柱结核患者作为研究对象,随机分为 CR组、 CT组、 MRI组,每组各 28例。对比分析三种检查方法在脊柱结核诊断中的临床价值。结果 CR组 28例患者中 19例 (67. 8% )患者的诊断结果符合脊椎结核的诊断标准; CT组 28例患者中 2 4例 (8 5.7% )患者的诊断结果符合脊椎结核的诊断标准;对 MRI组 28例患者的诊断结果均符合脊椎结核的诊断标准,三项检查之间比较无显著性差异 (P > 0.05 )。 结论 CR 、 CT 、 MRI 在脊柱结核诊断中均有较高的临床应用价值,建议临床检查时采用三者结合的方式进行诊断。
简介:Co(II)-salenwasencapsulatedinMIL-100(Cr)metalorganicframeworkby"shipinabottle"tosynthesizeanewelectrocatalyst,Cosalen@MIL-100(Cr).ThematerialwascharacterizedbyXRD,FT-IR,UV-VisandN2-adsorption.TheCosalen@MIL-100(Cr)modifiedglassycarbonelectrodeexhibitsawell-definedreductionpeakatthepotentialof–0.21Vtowardtheoxygenreductionreaction(ORR)bycyclicvoltammetry(CV)inpH=6.84phosphatebuffer.Almost400mVpositiveshiftofpotentialatCosalen@MIL-100(Cr)modifiedelectrodeforORRcomparedwiththatatbareglassycarbon,indicatesthatCosalen@MIL-100(Cr)possessesexcellentelectrocatalyticactivity.ThetransferrednumberofelectronsforORRwasdeterminedbychronocoulometry.TheresultsuggeststhattheintroductionofCo(II)-salencomplexintoMOFincreasestheelectrocatalyticactivityviaafour-electronreductionpathway.Furthermore,thiselectrocatalystexhibitsgoodstabilityandreproducibility.
简介:ExperimentshavebeenperformedonthesystemMgO-SiO2-Cr-Oat0-2.88GPaand1100-1450℃,focusingonthestabilityofCr^2+inolivine(O1),orthopyroxene(Opx)andspinel(Sp)anditspartitioningbetweenthesephases.Analyticalreagentgradechemicals,MgO,SiO2,Cr2O3.andCrwereusedtomakestartingmixtures.ExcessCr(50%)wasthenaddedinthesemixturestoensurethattheresultantphaseswereinequilibriumwiththemetalCr.FluxofBaO+B2O3(%)wasaddedforfacilitatingexperimentalequilibriumandcrystalgrowth.Crwasusedascapsulematerial.AllphasesintheproductwereidentifiedbyX-rayandanalyzedbyelectronmicroprobe,ThecontentsofCrOinthedifferentphases(O1,OpxandSp)werecalculatedaccordingtostoichiometry.TheobtainedresultsofcalculationindicatethatCr^3+inOlandOpxisnegligible.Theexperimentalresultsshow;(a)withincreasingtemperatureanddecreasingpressure,Cr^2+solubilityinOl,OpxandSpincreases;(b)withincreasingtemperature,thepartitioningcoefficientofMgandCr^2+betweenOlandOpxdecreases,thatbetweenOpxandSpincreases,andthatbetweenOlandSpremainsalmostunchanged;(c)theeffectofpressureonallpartitioningcoefficientsisnegligible.
简介:ArapidlysolidifiedAl-2.5Ti-2.5Fe-2.5Cr(massfractionin%)alloywaspreparedbymeltspinning.Asquenchedandas-annealedmicrostructureswerestudiedbyX-raydiffractometry(XRD),transmissionelectronmicroscopy(TEM),high-resolutiontransmissionelectronmicroscopy(HREM)andenergydispersivespectrum(EDS)analysis.Themicrohardnessofthealloyatdifferentannealingtemperatureswasmeasured.TheresultsobtainedindicatethatthemicrohardnessoftherapidlysolidifiedAl-2.5Ti-2.5Fe-2.5Cralloydoesnotvarywithdifferentannealingtemperatures.Theas-quenchedmicrostructureofthealloyincludestwokindsofdispersedprimaryphases:Al3TiandAl13(Cr,Fe)2.Afterannealingat400℃for10h,thestablephaseAl13Fe4appearsinthemicrostructure.